Istituto dei materiali per l'elettronica ed il magnetismo     
Mosca R., Ferro P., Calestani D., Nasi L., Besagni T., Licci F. Solvothermal synthesis of ZnS[C(2)H(4)(NH(2))(2)](0.5) nanosheets. In: Crystal Research and Technology, vol. 46 (8) pp. 818 - 822. WILEY-BLACKWELL 2011, 2011.
ZnS(en)(0.5) complex (en=ethylenediamine) can be synthesized by solvothermal route as thin sheet-like crystals using en as the single solvent. We studied the influence of the main synthesis parameters (i.e. temperature, pressure, time, reactant type and concentration) on the compound crystallization kinetics to achieve control on shape and dimensions of the ZnS(en)(0.5) nanoplatelets. We achieved a significant reduction of the platelet dimensions, while maintaining acceptable yield, by using a single piece of metal zinc as the Zn(2+) source.
URL: http://onlinelibrary.wiley.com/doi/10.1002/crat.201000690/abstract;jsessionid=4043B8C380587CD9CC0C81534BF79D56.d02t03
DOI: 10.1002/crat.201000690
Subject ZnS(ethylenediamine)
organic-inorganic hybrid
solvothermal synthesis

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